
Methyl 3-amino-4-methylthiophene-2-carboxylate determination of the content
Take 8.7g (0.05 mol) 3-carbonyl-4-methyl-tetrahydrothiophene-2-carboxylic acid methyl ester, add a certain amount of acetonitrile, stir and heat to reflux, then add 3.5g (0.05 mol) hydroxylamine hydrochloride to react.